This report shows the results of the research focused on the development of a procedure for the elaboration of optimized geopolymers; pretending to provide from this, a tool for future research in the field of alkaline activated cements; The tool by which the previous section is achieved consists of a procedure that allows geopolymers to be elaborated based on flying ash from the thermoelectric "TermoPaipa" inferred from a general evaluation of the behavior of this particular ash and the components of said geopolymer. to modify factors such as: forms, times and mixing equipment, as well as curing procedures, among others. In addition, research is relevant to the struggle proposed by all nations in the face of the problem of global warming, caused by the pollution of the environment. In the country, it is necessary to carry out research that provides tools to be at the forefront of the aforementioned issues. To achieve the purpose of the research, a laboratory methodology was chosen, in which an evaluation of the different procedures was carried out, in the different stages that can be followed to achieve a geopolymer, using previous research, the literature found, technical advice from the co-director and mixtures made in the laboratory. Based on the qualitative results obtained from the different procedures evaluated, the experimental results and the quantitative results obtained from the tests carried out on the processed specimens, it was possible to determine an optimal procedure for the preparation of geopolymers based on fly ash originating from the thermoelectric ThermoPaipa , which has unfavorable characteristics in geopolymerization processes such as the high contents of unburned organic material and very large particle sizes in relation to ashes cataloged as optimal for the preparation of geopolymers. Within the research, mixtures were made with the addition of industrial hemp fibers and with the implementation of a thermal treatment carried out on the fly ash; in order to optimize the mechanical properties of geopolymers, both compression and tension. The research produced results that were first synthesized in a procedure for obtaining geopolymers, which was optimized by modifications in times, use of superplasticizer, use of equipment and curing process; In addition, they were inferred as the main factors that affect the mechanical properties of geopolymers, the curing process and the process used to make the alkaline solution. Finally, an optimization of 54% was obtained in terms of the resistance to compression from a thermal treatment performed on the ash and up to 28% from the addition of industrial hemp fibers; In addition, the tensile strength was improved by 71% with the addition of said fiber. Through socialized research it was inferred that the ash produced by the thermoelectric "TermoPaipa" has a better behavior with the application of treatments that improve their physical properties, additionally it was determined that the use of hemp fiber contributes positively in the properties Mechanics of the geopolymers and finally it is necessary to clarify that each of the procedures evaluated and selected in this report had an impact on the feasibility of the geopolimeros elaboration.