Sodium hypochlorite has significant potential as a sanitation solution in hard-to-reach areas. Few studies have investigated the optimal electrolysis parameters for its production with volumes greater than 10 L. This study evaluated sodium hypochlorite production through electrolysis in a 22-L prototype and identified the optimal operating parameters. Tests were performed using graphite electrodes with areas of 68.4 cm 2 at the laboratory scale and 1 865.0 cm 2 at the prototype scale. A design for experiments with different operating times