In this work we report synthesis of the LaYbO3 ceramics material by the solid state reaction technique and its structural and morphological characterization from X-ray diffraction and Scanning Electron Microscopy experiments. Rietveld refinement of the diffraction patterns reveals that this material crystallizes in an orthorhombic perovskite, Pnma space group (#62) with lattice parameters a=6.0233Å, b=8.2080Å and c=5.7203Å. Systematic monitoring of the synthesis process is carried out through analysis of results of X-ray diffraction. The surface morphology of the samples was qualitatively analysed as a function of the sintering process.